Novel deprotection method of Fmoc group under neutral hydrogenation conditions
Novel deprotection method of Fmoc group under neutral hydrogenation conditions
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Publisher
Vienna: Vienna : Springer Vienna
Journal title
Language
English
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Publisher
Vienna: Vienna : Springer Vienna
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Scope and Contents
Contents
Novel deprotection method of the Fmoc (9-flurorenylmethoxycarbonyl) protective group under Pd/C-catalyzed hydrogenation conditions at room temperature was developed. The addition of CH₃CN accelerated the deprotection of the Fmoc group, and also the application of H₂ pressure (3 atm) shows notable rate enhancement.
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Full title
Novel deprotection method of Fmoc group under neutral hydrogenation conditions
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Record Identifier
TN_cdi_proquest_journals_1095699174
Permalink
https://devfeature-collection.sl.nsw.gov.au/record/TN_cdi_proquest_journals_1095699174
Other Identifiers
ISSN
0939-4451
E-ISSN
1438-2199
DOI
10.1007/s00726-008-0109-7
