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HPLC-DAD和LC-MS/MS法对各种芦荟样品中蒽醌类成分的分析研究

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HPLC-DAD和LC-MS/MS法对各种芦荟样品中蒽醌类成分的分析研究

https://devfeature-collection.sl.nsw.gov.au/record/TN_cdi_wanfang_journals_trcwyjykf200905023

HPLC-DAD和LC-MS/MS法对各种芦荟样品中蒽醌类成分的分析研究

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Full title

HPLC-DAD和LC-MS/MS法对各种芦荟样品中蒽醌类成分的分析研究

Author / Creator

陈欣霞 , 张宇航 , 林颖 , 谢志勇 and 万金志

Publisher

中山大学药学院药物分析实验室,广州,510006%珠海市第五人民医院,珠海,519000

Journal title

天然产物研究与开发, 2009, Vol.21 (5), p.817-848

Language

Chinese

Formats

Articles

Publication information

Publisher

中山大学药学院药物分析实验室,广州,510006%珠海市第五人民医院,珠海,519000

More information

Scope and Contents

Contents

R284.1%Q946; 采用HPLC-DAD和LC-MS/MS对各种芦荟样品中蒽醌类成分进行鉴定,在此基础上建立了同时测定各种芦荟样品中芦荟苷与芦荟大黄素含量的方法.采用Nucleodur-siliea色谱柱(250mm*4.6mm,5μm),流动相A为甲醇-醋酸(500:1.70),B为水-醋酸(500:1.70),梯度洗脱,流速1.0 mL/min,DAD扫描波长范围为190～370 nm,紫外检测波长为254和356 nm.质谱离子源为ESI,采用全扫描一级质谱和选择离子全扫描二级质谱两种方式同时测定.结果表明:各种芦荟样品中主要的蒽醌类成分为芦荟苷A、B与芦荟大黄素,未检测到大黄素、大黄酸、大黄素甲醚、大黄酚;芦荟干粉中所含的芦荟苷含量最高.该法准确、可靠、重现性好,可行性高.

Alternative Titles

Full title

HPLC-DAD和LC-MS/MS法对各种芦荟样品中蒽醌类成分的分析研究

Authors, Artists and Contributors

Author / Creator

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Primary Identifiers

Record Identifier

TN_cdi_wanfang_journals_trcwyjykf200905023

Permalink

https://devfeature-collection.sl.nsw.gov.au/record/TN_cdi_wanfang_journals_trcwyjykf200905023

Other Identifiers

ISSN

1001-6880

DOI

10.3969/j.issn.1001-6880.2009.05.023

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